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CALIXAR™ C2B Kit

CALIXAR™ C2B Crystallization Kit

Biological information

Background

This exciting new kit provides two varieties of stabilizing surfactants: Calixarenes 1-5 and fluorinated poly(tris) 6-8 and bis-glucose 9-11 surfactants. This new kit has been developed by CALIXAR SAS in partnership with the joint laboratory Chem2staB (C2B) at Avignon University, France. CALIXAR C2B derivatives have been designed & synthetized for their capacity to generate a network of salt bridges around the protein, in close proximity to the membrane domain with positively-charged residues located at the membrane-cytosol interface of the protein. They can also form a ‘cage’ around surface lysines, creating a ‘charge shield’. Fluorinated surfactants act in a very different manner to their hydrogenated equivalents due to the increased size of fluorine relative to hydrogen and its highly hydrophobic nature. Fluorinated surfactants are unable to extract proteins from the membrane, but can be useful in subsequent purification steps as they do not strip natural lipids and other co-factors from the proteins. In addition, the bulky fluorinated tailscannot penetrate into the interior and disrupt structure. Fluorinated surfactants often decrease non-specific aggregation and are thought to result in improved distribution on cryo-EM grids and better vitrification for cryo-EM data collection. They are also reported to increase crystallizability.

Target class
CALIXAR™ Crystallization Kit
Family
Accession number
Target Name
CALIXAR™ C2B Kit
Target Alias
Origin
Theori. MW
Affinity tag

Product specifications

Expression system
Purity
Purification method
Sample Buffer
Specified activity
Application
For Research Only
Storage conditions
Storage for the CALIXAR C2B Kit is 4°C (can be frozen at -20 ° C and heated up to 80°C).
Usage disclaimer
For Research Only

Chemical data

Background

This exciting new kit provides two varieties of stabilizing surfactants: Calixarenes 1-5 and fluorinated poly(tris) 6-8 and bis-glucose 9-11 surfactants. This new kit has been developed by CALIXAR SAS in partnership with the joint laboratory Chem2staB (C2B) at Avignon University, France. CALIXAR C2B derivatives have been designed & synthetized for their capacity to generate a network of salt bridges around the protein, in close proximity to the membrane domain with positively-charged residues located at the membrane-cytosol interface of the protein. They can also form a ‘cage’ around surface lysines, creating a ‘charge shield’. Fluorinated surfactants act in a very different manner to their hydrogenated equivalents due to the increased size of fluorine relative to hydrogen and its highly hydrophobic nature. Fluorinated surfactants are unable to extract proteins from the membrane, but can be useful in subsequent purification steps as they do not strip natural lipids and other co-factors from the proteins. In addition, the bulky fluorinated tailscannot penetrate into the interior and disrupt structure. Fluorinated surfactants often decrease non-specific aggregation and are thought to result in improved distribution on cryo-EM grids and better vitrification for cryo-EM data collection. They are also reported to increase crystallizability.

Compound name
CALIXAR™ Crystallization Kit
Catalog number
MD1-109
Molecular formula
CAS
nd
MW
2130 – 963.7 (g/mol)
Ka
na
Percent composition
CoA

Product specifications

Physical state
CALIXAR™ C2B Kit is presented as a 10 x 50 µL microfuge tubes of 3 x calixarene compounds, 6 x fluorinated and 1 x hydrogenated surfactants
Purity (HPLC 214nm)
CoA
Retention time (RP18 HPLC)
CoA
CMC
CoA
Exact mass
na
Stability
For Research Only
Solubility structure
Suggested working pH is between 6-9 to maintain solubility.
Datasheets
MD1-109
Datasheet
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